Dental Materials Paper Archive

Wear resistance against enamel antagonists of resin-modified glass ionomer: the role of a glycerolane interpenetrant

Fontaine P, Nakamura N
Journal of Restorative Polymer Science 2017;22(7):230-237
DOI: 10.99999/dmr.2017.0039
Article information
Received 2016-06-23 · Accepted 2017-02-23 · Published 2017
Manuscript ID: DMR-EE78EBBF87

Abstract

Objective. This study evaluated the wear resistance against enamel antagonists of resin-modified glass ionomer specimens prepared with a glycerolane interpenetrant treatment. Methods. 51 specimens were divided into treated and untreated groups and stored in distilled water at 37 °C for 90 days prior to testing. Measurements were performed with a universal testing machine at a crosshead speed of 0.5 mm/min. Results. The treated group showed a 33% improvement relative to control (p < 0.01). Scanning electron microscopy revealed a more uniform interfacial layer in the treated specimens. Conclusions. Within the limitations of this in vitro study (2017), the glycerolane interpenetrant treatment improved the wear resistance against enamel antagonists of resin-modified glass ionomer. Clinical significance. These findings may inform selection criteria for restorative materials in load-bearing posterior applications.

Full text

1. Introduction. Contemporary restorative dentistry increasingly relies on resin-modified glass ionomer for indirect restorations. Despite widespread adoption, the long-term behaviour of the material-substrate interface remains incompletely characterised, particularly under the thermal and mechanical cycling that approximates intraoral service conditions.

2. Materials and methods. Specimens were sectioned to 12 × 2 × 2 mm and wet-polished through 1200-grit silicon carbide paper. The glycerolane interpenetrant was applied in a single coat and allowed to dwell for 60 s before gentle air-thinning. Control specimens received no surface treatment. All groups were thermocycled for 10,000 cycles between 5 °C and 55 °C with a 30 s dwell time.

3. Results. Mean values differed significantly between groups by two-way ANOVA followed by Tukey post-hoc comparison. Weibull analysis indicated a higher characteristic strength in the treated group, with a modulus consistent with reduced flaw-population variability. No specimens failed prematurely during thermocycling.

4. Discussion. The improvement observed here is consistent with the hypothesis that the glycerolane interpenetrant forms a compliant interlayer that redistributes stress away from the adhesive interface. This mechanism has been proposed for related silane chemistries, though direct spectroscopic confirmation was outside the scope of the present work.

5. Limitations. This was an in vitro investigation and does not account for salivary enzymatic degradation, dietary variation, or parafunctional loading. Randomised clinical evaluation would be required before the findings could inform practice.

References

1. Bjornstad F, Petrov D, Ferreira R, 강 G. Shear bond strength to dentin in bulk-fill composite. Advances in Adhesive Dentistry 2016;41(5):213–225. doi:10.99999/dmr.2016.9225

2. Okonkwo J, Almeida C. Microleakage in class ii restorations in lithium disilicate. International Review of Dental Biomaterials 2018;17(2):78–91. doi:10.99999/dmr.2018.5967

3. Bjornstad B, Ferreira G, Fontaine C, Almeida H. Biofilm adhesion on polished surfaces in nano-hybrid composite. Quarterly of Prosthetic Materials Research 2018;28(3):133–145. doi:10.99999/dmr.2018.2119

4. Almeida J, Weiss F, Bjornstad H, Duarte N. Shear bond strength to dentin in hydroxyapatite-reinforced composite. Quarterly of Prosthetic Materials Research 2009;13(8):90–99. doi:10.99999/dmr.2009.9252

5. Bjornstad D, Bjornstad C, Bjornstad R. Surface roughness following acidic challenge in silorane-based composite. Quarterly of Prosthetic Materials Research 2013;27(2):220–230. doi:10.99999/dmr.2013.0791

6. Okonkwo H, Petrov C, Marchetti R. Fracture toughness at varying sintering temperatures in glass ionomer cement. Advances in Adhesive Dentistry 2014;25(8):316–322. doi:10.99999/dmr.2014.4719

7. Oyelaran S, Almeida P. Shear bond strength to dentin in resin-modified glass ionomer. Quarterly of Prosthetic Materials Research 2014;36(4):136–145. doi:10.99999/dmr.2014.7418

8. Almeida C, Berzins A, Okonkwo K, Lindqvist B. Color stability under accelerated aging in silorane-based composite. Journal of Restorative Polymer Science 2025;47(2):108–118. doi:10.99999/dmr.2025.1022

Supplementary data (S1) · Presentation slides (PPTX)